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糖醛酸半微量测定方法的改进
Improvement of Semimicro Determination of Uronic Acids
【摘要】 <正> 纸浆中糖醛酸含量的多少,与纸浆的打浆和成纸的性能有着重要的关系。同一种原料,亚硫酸盐法浆与硫酸盐法浆的差别,在很大程度上也与糖醛酸的含量有关。因此测定纸浆中糖醛酸的含量应当得到重视。 纸浆中糖醛酸含量的测定,除了应用液相色谱法作微量分析外,可以用化学方法作半微量测定。化学方法的原理是用强酸使糖醛酸脱
【Abstract】 The Johansson’s method for determination of the uronic acid content in raw materials or pulps is very complicate, though it is a volumetric method. Our improved method is based upon the decarboxylation of the uronic acids with 12% hydrochloric acid and the carbon dioxide evolved is absorbed with quantitative barium hydroxide solution. The excessive barium hydroxide is titrated directly with standard oxalic acid solution. The uronic acid content can be calculated in comparison with the blank test.
- 【文献出处】 中国造纸 ,China Pulp & Paper , 编辑部邮箱 ,1982年02期
- 【被引频次】1
- 【下载频次】54